Page 89 - CatalogNEP-LS

PRACTICAL (30 Hours)

1. Systematic Qualitative Organic Analysis of Organic Compounds possessing monofunctional
groups (-COOH, phenolic, aldehydic, ketonic, amide, nitro, amines) and preparation of one
derivative.
2. Organic Synthesis:
(i) Preparation of Iodoform.
(ii) Preparation of p-bromoacetanilide from acetanilide.
(iii)Preparation of glucosazone.
(iv) Preparation of aspirin.
3. Thin Layer Chromatography
(i) Determination of R f value and purity of organic compounds by use of thin layer
chromatography.
(ii) To analyze the organic compounds by thin layer chromatography.

SUGGUESTED READINGS:

1. Principles of Physical Chemistry by Puri, Sharma and Pathania.
2. Physical Chemistry by S.C. Khetarpal, G.S, Sharma and R.K. Kalia.
3. Moderns Approach to Physical Chemistry by S. Kiran.
4. A text Book of Physical Chemistry by K.K.Sharma and I.K. Sharma
5. Physical Chemistry by P.N.Kapil and S.K.Guglani.
6. Elements of Physical Chemistry by Puri, Sharma and Pathania.
7. Advance Organic Chemistry Reaction Mechanism and Structure by Jerry March.
8. Organic Chemistry by SM Mukherji, SP Singh and RP Kapoor, Vol. I, II & III, New Age
International Publishers
9. Organic Chemistry (Volume II) by I. L Finar

Chem.321 Chemical Thermodynamics and Electrochemistry 3+1

LEARNING OBJECTIVES:

The learning objectives: of this course are as follows:

• To provide basic knowledge about the heat changes taking place during various chemical
and physical changes.
• To familiarise the students about the basic concepts of electrical conductivity.

LEARNING OUTCOMES:

By the end of this course, students will be able to:
 apply the fundamental concepts of energy changes taking place in the universe
 Understand the phenomena involved in conductance measurements and its applications.
UNIT-I: (10Hours)
Chemical Thermodynamics: Review of thermodynamics First Law of Thermodynamics,
statement, definition of internal energy and enthalpy. Heat capacity, heat capacities at constant
volume and pressure and their relationship. Joule‘s law, Joule-Thomson coefficient, and inversion
temperature. Calculation of w, q, dU & dH for the expansion of ideal gases under isothermal and
adiabatic conditions for reversible process.

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